HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 7183144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 66756758 | HCID 66756758 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 7183144 | HCID 7183144 | — |
Reaction Steps
To a stirred solution of (1-(4-chloro-benzoyl)-piperidin-4-yl)-carbamic acid tert-butyl ester (46 g, 0.23 mmol) in CH2Cl2 (0.5 mL) was added trifluoroacetic acid (0.5 ml). The reaction mixture was stirred at room temperature for ½ hour. The reaction mixture was concentrated under reduced pressure to provide the titled compound. MS (DCI) m/z 239 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07262207B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-46390b43d7eb4c07a6598ee617cfce79 |
| Source note | uspto-grants-2007_08 |