Propanal → N,N-Bis(2-methylpropyl)prop-1-en-1-amine

HRID 856841Notes

Reaction equation

[CH:1](=O)[CH2:2][CH3:3].[CH2:5]([NH:9][CH2:10][CH:11]([CH3:13])[CH3:12])[CH:6]([CH3:8])[CH3:7]>>[CH2:5]([N:9]([CH:1]=[CH:2][CH3:3])[CH2:10][CH:11]([CH3:13])[CH3:12])[CH:6]([CH3:8])[CH3:7]

Participants

Reactant 2

HCID 527Propanal

HCID 8085Diisobutylamine

Product 1

HCID 54063094N,N-Bis(2-methylpropyl)prop-1-en-1-amineYield 29%

Procedure

Following a procedure similar to that described in Example 64(i), but using propionaldehyde and diisobutylamine as starting materials, the title compound was obtained as a colorless oily substance (yield 29%), boiling at 63-66° C./10 mmHg

Sources & evidence

ORD record: ord-9f7f5cf3cde04a918e833f98051f0231
Source dataset: uspto-grants-2006_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: USRE039420E1

Reaction notes

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