Sulfanilamide → N,N-Bis(2-methylpropyl)prop-1-en-1-amine

HRID 856842Notes

Reaction equation

HRID 856842 reaction equation
ClC1C=CC(C(=O)[CH2:7][CH:8]([CH3:11])[CH:9]=O)=CC=1.S(C1[CH:25]=[CH:24][C:22]([NH2:23])=CC=1)(=O)(=O)N>>[CH2:7]([N:23]([CH:22]=[CH:24][CH3:25])[CH2:9][CH:8]([CH3:7])[CH3:11])[CH:8]([CH3:11])[CH3:9]

Participants

3

Reactant 2

HCID 5333SulfanilamideHCID 21862891HCID 21862891, compound

Product 1

HCID 54063094N,N-Bis(2-methylpropyl)prop-1-en-1-amine

Procedure

Following a procedure similar to that described in Example 64(iii), but using 2-(4-chlorophenacyl) propionaldehyde [prepared as described in step (ii) above] and 4-sulfamoylaniline as starting materials, the title compound was obtained as a pale brown powder (yield 35%), melting at 196-198° C.

Sources & evidence

ORD record
ord-fa19c9d871d2448f997d265c8f3c0644
Source dataset
uspto-grants-2006_12
Patent number
USRE039420E1

Reaction notes

Loading…