Sulfanilamide → HCID 21862874, compound

HRID 856845Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][C:4]=1[CH3:11].[S:12]([C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1)(=[O:15])(=[O:14])[NH2:13]>>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=[N:20][C:19]2[CH:21]=[CH:22][C:16]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:17][CH:18]=2)=[CH:5][C:4]=1[CH3:11]

Participants

Reactant 2

HCID 5333Sulfanilamide

HCID 1229363-Methyl-4-anisaldehyde

Product 1

HCID 21862874HCID 21862874, compound

Procedure

Following a procedure similar to that described in Example 1(i), but using 4-methoxy-3-methylbenzaldehyde and 4-sulfamoylaniline as starting materials, the title compound was obtained as a yellow powder (yield 92%).

Sources & evidence

ORD record: ord-b1c91c22ccff4b06b88aefe65e7dbaa6
Source dataset: uspto-grants-2006_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: USRE039420E1

Reaction notes

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