4-(Methylthio)aniline → 4-Methylthio-N-(4-sulfamoylbenzylidene)aniline
Reaction equation
[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2].[CH3:13][S:14][C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1>>[CH3:13][S:14][C:15]1[CH:21]=[CH:20][C:18]([N:19]=[CH:9][C:8]2[CH:11]=[CH:12][C:5]([S:1](=[O:4])(=[O:3])[NH2:2])=[CH:6][CH:7]=2)=[CH:17][CH:16]=1Participants
3
Procedure
Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-methylthioaniline as starting materials, the title compound was obtained as a yellow powder (yield 95%).
Sources & evidence
- ORD record
- ord-5db54ffa57ca49fda3000641d224dc65
- Source dataset
- uspto-grants-2006_12
- Patent number
- USRE039420E1
Reaction notes
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