3,4-Dimethylaniline → HCID 21862755, compound
Reaction equation
[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2].[CH3:13][C:14]1[CH:15]=[C:16]([CH:18]=[CH:19][C:20]=1[CH3:21])[NH2:17]>>[CH3:13][C:14]1[CH:15]=[C:16]([CH:18]=[CH:19][C:20]=1[CH3:21])[N:17]=[CH:9][C:8]1[CH:11]=[CH:12][C:5]([S:1](=[O:4])(=[O:3])[NH2:2])=[CH:6][CH:7]=1Participants
3
Procedure
Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 3,4-dimethylaniline as starting materials, the title compound was obtained as a yellow powder (yield 60%).
Sources & evidence
- ORD record
- ord-8ea6c6750b454e8cbd76b2de3457963e
- Source dataset
- uspto-grants-2006_12
- Patent number
- USRE039420E1
Reaction notes
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