Sodium Hydroxide → HCID 21867190, compound

Participants

Reaction Conditions

Reaction Steps

A solution of ethyl N-{[(3-iodobenzyl)amino]carbonyl}glycinate (7.6 g) in MeOH (40 ml) was treated with aqueous 2M NaOH (21.2 ml) and stirred under nitrogen at 20° C. The mixture crushed out instantly and was quenched by adding aqueous 2M HCl (22 ml). The residue was filtered to give the title compound (4.4 g) LCMS=2.73 min.

Provenance & Evidence