HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium Chloride → 2-Chloro-4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium Chloride | HCID 24293 | — |
| Reactant | 4-[6-(4-Trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazol-2-ylamine | HCID 10091650 | — |
| Catalyst | Cuprous chloride | HCID 62652 | — |
| Product | 2-Chloro-4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazole | HCID 10476517 | — |
Reaction Steps
The title compound was prepared in an analogous manner to the conditions of Example 91 by reacting 4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazol-2-ylamine (Example 65) with CsCl and CuCl. MS (ESI, pos. ion.) m/z: 408 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144888B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-d5a40e3dd74b44f0bbeb53c35f3a7969 |
| Source note | uspto-grants-2006_12 |