HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethanol → 3-(2-hydroxyethyl)-1,2,3-benzotriazin-4(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethanol | HCID 10898 | — |
| Reactant | 1,2,3-Benzotriazin-4(1H)-one | HCID 135408793 | — |
| Product | 3-(2-hydroxyethyl)-1,2,3-benzotriazin-4(3H)-one | HCID 3780028 | — |
Reaction Steps
3-(2-hydroxyethyl)-1,2,3-benzotriazin-4(3H)one was prepared according to the general procedure outlined in example 1, step 1. Starting from 1,2,3-benzotriazin-4(3H)one (1.5 g, 10 mmol) and 2-bromoethanol (1.68 mL, 20 mmol), 1.20 g (63%); off white solid; m.p. 114° C., MS: 191.9 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148235B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-5e651ec973994eb496d1ed7f19535e57 |
| Source note | uspto-grants-2006_12 |