HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-3-iodopropane → HCID 11075029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-3-iodopropane | HCID 81363 | — |
| Reactant | 1,2,3-Benzotriazin-4(1H)-one | HCID 135408793 | — |
| Product | HCID 11075029 | HCID 11075029 | — |
Reaction Steps
3-(3-chloropropyl)-1,2,3-benzotriazin-4(3H)one was prepared according to the general procedure outlined in example 6, step 1. Starting from 1,2,3-benzotriazin-4(3H)one (2 g, 13.6 mmol) and 1-chloro-3-iodopropane (1.6 mL, 14.95 mmol), 1.57 g (52%); yellow solid; m.p. 69° C., MS: 223.9 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148235B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-8ece5ebbde11416eb52f0e1bbf7c2b8d |
| Source note | uspto-grants-2006_12 |