p-Anisoyl chloride → HCID 135546593, compound

HRID 858228Notes

Reaction equation

HRID 858228 reaction equation
[Cl:1][C:2]1[C:8]([O:9]C)=[CH:7][C:5]([NH2:6])=[C:4]([O:11][CH3:12])[CH:3]=1.C[O:14][C:15]1[CH:23]=[CH:22][C:18](C(Cl)=O)=[CH:17][CH:16]=1>>[Cl:1][C:2]1[C:8]([OH:9])=[CH:7][C:5]2[N:6]=[C:12]([C:18]3[CH:22]=[CH:23][C:15]([OH:14])=[CH:16][CH:17]=3)[O:11][C:4]=2[CH:3]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 228334-Chloro-2,5-dimethoxyaniline

Product 1

HCID 135546593HCID 135546593, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 16, from 4-chloro-2,5-dimethoxyaniline, and 4-methoxybenzoyl chloride and was obtained as an off-white solid, m.p. 260–262° C.; MS m/e 260 (M−H)+.

Workup

  1. customwas obtained as an off-white solid, m.p. 260–262° C.

Sources & evidence

ORD record
ord-e3fa63d7aac54a7484f42ed17762362e
Source dataset
uspto-grants-2006_12
Patent number
US07148247B2

Reaction notes

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