HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyldimethylsilyl chloride → HCID 11387060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | 7-Bromo-5-methoxy-2-(4-methoxyphenyl)-1,3-benzoxazole | HCID 12148969 | — |
| Product | HCID 11387060 | HCID 11387060 | — |
Reaction Steps
The title compound was prepared in substantially the same manner as described in Example 24, Route a, Step a, from 7-bromo-5-methoxy-2-(4-methoxyphenyl)-1,3-benzoxazole, and tert-butyl(chloro)dimethylsilane. The desired product was obtained as a white solid, m.p. 90–91° C.; MS m/e 534 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148247B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-e343750b50f747c0b3727b8406927ab1 |
| Source note | uspto-grants-2006_12 |