HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-2-methylbenzoic acid → 7-Bromo-2-(4-hydroxy-2-methylphenyl)benzo[d]oxazol-5-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-2-methylbenzoic acid | HCID 597216 | — |
| Reactant | 2-Amino-6-Bromo-4-Methoxyphenol | HCID 11171982 | — |
| Product | 7-Bromo-2-(4-hydroxy-2-methylphenyl)benzo[d]oxazol-5-ol | HCID 135483640 | — |
Reaction Steps
The title compound was prepared in substantially the same manner as described in Example 21, from 4-methoxy-2-methylbenzoic acid, and 2-amino-6-bromo-4-methoxyphenol, and was obtained as a light purple solid, m.p. 120–135° C.; MS m/e 320 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148247B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-50304db9b7914bcc9edf6d51bebacae6 |
| Source note | uspto-grants-2006_12 |