HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenol → 3-Bromo-5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenol | HCID 7244 | — |
| Reactant | Hexane, 2,5-dichloro-2,5-dimethyl- | HCID 80360 | — |
| Product | 3-Bromo-5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-ol | HCID 10779311 | 78.4% |
Reaction Steps
In a manner similar to that of Example 36(a), by reaction of 67.14 g (388.0 mmol) of 2-bromophenol with 71.10 g (388.0 mmol) of 2,5-dichloro-2,5-dimethylhexane, 86.13 g (78%) of the expected product are obtained in the form of a white solid with a melting point of 90–94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148245B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-67f63e38947a4e5a88e855729bbc17db |
| Source note | uspto-grants-2006_12 |