4-Aminophenethyl alcohol → HCID 21876435, compound

HRID 858464Notes

Reaction equation

HRID 858464 reaction equation
[Cl:1][C:2]1[CH:9]=[C:8](Cl)[C:7]([N+:11]([O-:13])=[O:12])=[CH:6][C:3]=1[C:4]#[N:5].[NH2:14][C:15]1[CH:20]=[CH:19][C:18]([CH2:21][CH2:22][OH:23])=[CH:17][CH:16]=1>>[Cl:1][C:2]1[CH:9]=[C:8]([NH:14][C:15]2[CH:20]=[CH:19][C:18]([CH2:21][CH2:22][OH:23])=[CH:17][CH:16]=2)[C:7]([N+:11]([O-:13])=[O:12])=[CH:6][C:3]=1[C:4]#[N:5]

Participants

3

Reactant 2

HCID 669044-Aminophenethyl alcoholHCID 218763462,4-Dichloro-5-nitrobenzonitrile

Product 1

HCID 21876435HCID 21876435, compound

Procedure

The title compound was prepared according to the procedure described in step 3 of Example 1 from 2,4-dichloro-5-nitrobenzonitrile (Grivsky, E. M.; Hitchings, G. H. Ind. Chim. Belge., 1974, 39. 490.) and 4-aminophenylethyl alcohol.

Sources & evidence

ORD record
ord-203f288f961443b0b4b34137ca9d810a
Source dataset
uspto-grants-2006_12
Patent number
US07148234B2

Reaction notes

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