HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-[2-(5-Chloro-2,4-dimethoxy-phenyl)ethyl]-6-cyclopentyl-tetrahydropyran-2,4-dione → HCID 136152594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-[2-(5-Chloro-2,4-dimethoxy-phenyl)ethyl]-6-cyclopentyl-tetrahydropyran-2,4-dione | HCID 16728701 | — |
| Reactant | 2-(bromomethyl)quinazolin-4(1h)-one | HCID 135454034 | — |
| Product | HCID 136152594 | HCID 136152594 | 19% |
Reaction Steps
The title compound was prepared as described in Example B(53), using 2-(bromomethyl)-quinazolin-4(3H)-one (Example B(55), Step 1) in place of 5-(chloromethyl)-1,3-dimethyl-1H-1,2,4-triazole, and using 6-[2-(5-chloro-2,4-dimethoxyphenyl)ethyl]-6-cyclopentyldihydro-2H-pyran-2,4(3H)-dione in place of 6-[2-(3-chloro-4-methoxyphenyl)ethyl]-6-cyclopentyldihydro-2H-pyran-2,4(3H)-dione. Yield: 19%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148226B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-c2d3351316b0420eb46a51437d71b315 |
| Source note | uspto-grants-2006_12 |