3-Ethoxy-2-methylacrylaldehyde → HCID 178430151, compound
Reaction equation
CCO/[CH:4]=[C:5](/[CH:7]=O)\[CH3:6].[NH2:9][C:10]1[N:14]=[C:13]([SH:15])[NH:12][N:11]=1>>[CH3:6][C:5]1[CH:4]=[N:9][C:10]2[N:11]([N:12]=[C:13]([SH:15])[N:14]=2)[CH:7]=1Participants
3
Procedure
The title compound was prepared from 3-ethoxymethacrolein and 3-amino-5-mercapto-1,2,4-triazole as previously described by M. Künstlinger and E. Breitmaier in Synthesis, 1983, 44–47.
Workup
- customBreitmaier in Synthesis, 1983, 44–47
Sources & evidence
- ORD record
- ord-be7a4dd7f6e44312a57a25dcea4a30ba
- Source dataset
- uspto-grants-2006_12
- Patent number
- US07148226B2
Reaction notes
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