Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 2-chloroacetoacetate → HCID 58762430, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 2-chloroacetoacetate | HCID 107332 | — |
| 반응물 | 1-Cyclopentyl-5-(4-hydroxy-2,5-dimethyl-phenyl)-pent-4-yn-1-one | HCID 58762502 | — |
| 반응물 | HCID 58762649 | HCID 58762649 | — |
| 생성물 | HCID 58762430 | HCID 58762430 | — |
반응 단계
The desired product was prepared analogously to example F(1), Step 2, substituting N-(3-cyclopentyl-3-oxo-propyl)-3-furan-2-yl-propionamide (300 mg, 1.1 mmol) from Step 2 above in place of 1-cyclopentyl-5-(4-hydroxy-2,5-dimethyl-phenyl)-pent-4-yn-1-one and methyl 2-chloroacetoacetate (0.7 mL, 5.7 mmol) in place of methyl acetoacetate. Yield: 103 mg, 14%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07148226B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-7ceb2146659b4a63a27fde9c4efa81c1 |
| 출처 메모 | uspto-grants-2006_12 |