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HRID859285

反应详情

EQUATION

反应方程式

HRID 859285 的结构方程式

REACTANTS

反应物

2
结构：[CH3][Sn]([CH3])([CH3])[c]1ccc(OCc2ccccc2)nc1
HCID22224741

未命名化合物

结构：CC(C)(C)OC(=O)Nc1ccc(I)cc1[N+](=O)[O-]
HCID23554339

Tert-butyl (4-iodo-2-nitrophenyl)carbamate

C11H13IN2O4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1ccc(-c2ccc(OCc3ccccc3)nc2)cc1[N+](=O)[O-]
HCID69592778

未命名化合物

收率 103.9%

PROCEDURE

实验过程

Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1) (728 mg, 2.0 mmol) and 2-(phenylmethoxy)-5-(trimethylstannyl)-pyridine (766 mg, 2.2 mmol) [CAS-No. [188881-22-3], WO 9709311] according to the general procedure E. Obtained as a yellow solid (876 mg).