HCID 22224698, compound → HCID 69592853, compound

HRID 859364Notes

Reaction equation

HRID 859364 reaction equation
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[C:7]1[CH:8]=[C:9]([CH:15]=[CH:16][CH:17]=1)[C:10]([O:12]CC)=O.[C:18]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])(=[O:20])[CH3:19].[Li]>>[C:22]([O:21][C:18](=[O:20])[CH2:19][C:10]([C:9]1[CH:15]=[CH:16][CH:17]=[C:7]([C:3]2[N:2]([CH3:1])[CH:6]=[CH:5][N:4]=2)[CH:8]=1)=[O:12])([CH3:25])([CH3:24])[CH3:23]

Participants

3

Reactant 2

HCID 22224698HCID 22224698, compoundHCID 86586795Lithium Tert-butyl Acetate

Product 1

HCID 69592853HCID 69592853, compound

Procedure

Prepared from ethyl 3-(1-methyl-1H-imidazol-2-yl)benzoate [CAS-No. 168422-44-4] by treatment with lithium tert.-butyl acetate according to general procedure H (method b). Obtained as a light yellow liquid (1.26 g).

Sources & evidence

ORD record
ord-eea453e94cef48e297440fffacc1dc71
Source dataset
uspto-grants-2006_12
Patent number
US07151098B2

Reaction notes

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