Silver Nitrate → HCID 178418580, compound

HRID 859813Notes

Reaction equation

HRID 859813 reaction equation
[N+]([O-])([O-])=O.[Ag+:5].[NH:6]1[C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][C:9]=2[N:8]=[N:7]1.[Na]>O>[NH:6]1[C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][C:9]=2[N:8]=[N:7]1.[Ag:5]

Participants

4

Reactant 2

HCID 24470Silver NitrateHCID 178507076HCID 178507076, compound

Product 1

HCID 178418580HCID 178418580, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A dispersion of silver benzotriazole was prepared by concurrently adding a solution of silver nitrate, and a solution of sodium benzotriazole into a stirred aqueous bone gelatin solution. The small particle dispersion was centrifuged and the solid phase was resuspended in water, treated with a protolytic enzyme at 35° C. to destroy the gelatin, centrifuged, washed with water, resuspended in water, sonicated, and finally freeze-dried to a free-flowing white powder.

Workup

  1. additiontreated with a protolytic enzyme at 35° C.
  2. customto destroy the gelatin
  3. washwashed with water
  4. customsonicated
  5. customfinally freeze-dried to a free-flowing white powder

Sources & evidence

ORD record
ord-e28c532273fc46a8926572c59c281799
Source dataset
uspto-grants-2006_12
Patent number
US07153635B1

Reaction notes

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