Tetraethylammonium Hydroxide → HCID 86760339, compound

HRID 859815Notes

Reaction equation

HRID 859815 reaction equation
[C:1]([OH:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[OH-].[CH2:26]([N+:28]([CH2:33][CH3:34])([CH2:31][CH3:32])[CH2:29][CH3:30])[CH3:27]>O>[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[CH2:26]([N+:28]([CH2:33][CH3:34])([CH2:31][CH3:32])[CH2:29][CH3:30])[CH3:27]

Participants

4

Reactant 2

HCID 6509Tetraethylammonium Hydroxide2×HCID 8215Docosanoic Acid

Product 1

HCID 86760339HCID 86760339, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
70 °C

Procedure

A mixture of 100 g water, 8.95 g of behenic acid (20 mmole), and 8.0 g of a 35 weight % solution of tetraethylammonium hydroxide was heated to 70° C. with stirring. Then an additional 0.16 g of the tetraethylammonium hydroxide solution was added to adjust the pH to 8.3 (˜20 mmole total). The resulting opalescent solution was freeze dried to yield a white free-flowing powder.

Workup

  1. customdried
  2. customto yield a white free-flowing powder

Sources & evidence

ORD record
ord-2132300be16c4c88ae9828826e80f518
Source dataset
uspto-grants-2006_12
Patent number
US07153635B1

Reaction notes

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