HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydroxybenzoic Acid → HCID 178463981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydroxybenzoic Acid | HCID 19 | — |
| Reactant | Tetraethylammonium Hydroxide | HCID 6509 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178463981 | HCID 178463981 | — |
Reaction Steps
To 20 g of water and 3.08 g of 2,3-dihydroxybenzoic acid (20 mmole) at 20° C. was added a 35 weight % solution of tetraethylammonium hydroxide to adjust the pH to 7.9 (8.1 g required, ˜20 mmole). The resulting solution was freeze dried to yield a tan colored free-flowing powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153635B1 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-96ffed1a00834cce918ece62135552db |
| Source note | uspto-grants-2006_12 |