HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 15710569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 2,4-Pyrrolidinedione | HCID 551491 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15710569 | HCID 15710569 | — |
Reaction Steps
A solution of pyrrolidin-2,4-dione (6.93 g, 70 mmol) produced in step 1 and 1,2-phenylenediamine (7.88 g, 70 mmol) in methanol was stirred at 60° C. for 1 hour. The reaction solution was cooled, and the crystals thus formed were taken by the filtration to synthesize 4-((2-aminophenyl)amino)-3-pyrrolin-2-one (yield: 11.6 g, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153850B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-cc872629ef0c4dabbb8a376b1b66c794 |
| Source note | uspto-grants-2006_12 |