1,4-Dioxane hydrochloride → HCID 23435534, compound

Participants

Reaction Steps

To a solution of 4-2 (2.18 g, 4.45 mmol) in dichloromethane (5.0 mL) at room temperature under Ar was added 4.0 M HCl-dioxane solution (25 mL). A white precipitate formed immediately. After two hours the reaction was concentrated and dried to yield a white solid;

Provenance & Evidence