HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 860071Generated: October 30, 2026
Sodium Hydroxide → HCID 10111379, compound
https://huagongshe.com/reaction/860071
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 58765553 | HCID 58765553 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10111379 | HCID 10111379 | — |
Reaction Steps
To a solution of 8-14 (0.50 g, 1.36 mmol) in ethanol (10 mL) was added 1N NaOH (1.5 mL), and the mixture stirred at 50° C. for 30 minutes, then concentrated. The residue was chromatographed on silica gel (25:10:1:1 to 15:10:1:1 EtOAc/EtOH/NH4OH/H2O) to give 8-15 as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07153862B2 |
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| Source dataset | uspto-grants-2006_12 |
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| ORD ID | ord-ae10dfe178fa4c6b96d2a3b26308794f |
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| Source note | uspto-grants-2006_12 |
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