HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178418850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Aminopyrimidine | HCID 7978 | — |
| Reactant | Cyclohexyl isocyanide | HCID 79129 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 178418850 | HCID 178418850 | — |
Reaction Steps
Example 6 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153873B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-5a3f58d8d6c543708c83bb8200d6c370 |
| Source note | uspto-grants-2006_12 |