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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 860117Generated: October 30, 2026

Benzaldehyde → HCID 178419071, compound

https://huagongshe.com/reaction/860117

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
ReactantOctanoyl chlorideHCID 8124—
Reactant2-AminopyridineHCID 10439—
ReactantTert-Butyl isocyanideHCID 23577—
SolventPerchloric AcidHCID 24247—
ProductHCID 178419071HCID 178419071—

Reaction Steps

Example 11 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process steps b) to d) by reacting the resultant reaction product with 0.4 mmol heptylcarboxylic acid chloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07153873B2
Source datasetuspto-grants-2006_12
ORD IDord-6032497b96ac442e95fd3ef6a895b3b6
Source noteuspto-grants-2006_12