HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 3-(4-Fluoro-phenyl)-2-methyl-5-(2-methyl-pyridin-4-ylethynyl)-3H-imidazole-4-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 4-[1-(4-Fluoro-phenyl)-2-methyl-1H-imidazol-4-ylethynyl]-2-methyl-pyridine | HCID 10085660 | — |
| Product | 3-(4-Fluoro-phenyl)-2-methyl-5-(2-methyl-pyridin-4-ylethynyl)-3H-imidazole-4-carbaldehyde | HCID 10064532 | — |
Reaction Steps
3-(4-Fluoro-phenyl)-2-methyl-5-(2-methyl-pyridin-4-ylethynyl)-3H-imidazole-4-carbaldehyde (89) [MS: m/e=320.4 (M+)] was prepared in analogy to the method as above from 4-[1-(4-Fluoro-phenyl)-2-methyl-1H-imidazol-4-ylethynyl]-2-methyl-pyridine (1) and N,N-dimethyl-formamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153874B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-4d35909819ba496d990c87561fbb50e4 |
| Source note | uspto-grants-2006_12 |