Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(Phenylacetyl)-L-alanine → 3-(N'-(Phenylacetyl)-alaninyl)amino-epsilon-caprolactam
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| 반응물 | 4-Aminoazepan-2-one | HCID 21584138 | — |
| 생성물 | 3-(N'-(Phenylacetyl)-alaninyl)amino-epsilon-caprolactam | HCID 10215097 | — |
반응 단계
Following General Procedure B above using N-(phenylacetyl)-L-alanine (Example A) and 3-amino-ε-caprolactam (Sigma), the title compound was prepared as a solid having a melting point of 200–202° C. The reaction was monitored by tlc on silica gel (Rf=0.30 in 1:9 methanol/dichloromethane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07153847B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-8704abe6fb384f8ab68938571121a23b |
| 출처 메모 | uspto-grants-2006_12 |