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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 860284Generated: October 31, 2026

HCID 22312692, compound → HCID 86584980, compound

https://huagongshe.com/reaction/860284

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22312692HCID 22312692—
ReactantHCID 23552772HCID 23552772—
ProductHCID 86584980HCID 86584980—

Reaction Steps

Following General Procedure I above using cyclopentyl-α-hydroxyacetic acid (Example P) and 3-(L-alaninyl)-amino-2,4-dioxo-1,5-bis-phenyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine hydrochloride (Example 8-W), the title compound was prepared as a white solid (melting point=139–1,49° C.). Purification was by flash chromatography eluting with CH2Cl2/EtOAc (1:2). Rf=0.50 and 0.39 (CH2Cl2/EtOAc, 1:2).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07153847B2
Source datasetuspto-grants-2006_12
ORD IDord-a3d427f405f84120bef131bc627dccf4
Source noteuspto-grants-2006_12