HCID 67104648, compound → HCID 67104656, compound

Participants

Reaction Steps

Methanesulfonic acid 2-[6-(2,6-dimethyl-pyridin-3-yl)-naphthalen-2-yl]-ethyl ester The compound was prepared by the method in Example 3B substituting 2-[6-(2,6-dimethyl-pyridin-3-yl)-naphthalen-2-yl]-ethanol in place of 4-[6-(2-hydroxy-ethyl)-naphthalen-2-yl]-benzonitrile (0.9763 g, 97% yield). 1H NMR (CD3OD, 300 MHz), δ 8.09–8.05 (m, 1H), 7.99–7.87 (m, 2H), 7.82–7.79 (m, 1H), 7.66–7.62 (m, 1H), 7.53–7.44 (m, 2H), 7.22–7.13 (m, 1H), 4.57–4.52 (t, J=7.5 Hz, 2H), 4.08 (s, 3H), 3.27–3.19 (t, J=7.5 Hz, 2H). MS (DCI-NH3) [M+H]+ at 356.

Provenance & Evidence