4-Nitrophenol → HCID 69374630, compound

HRID 860998Notes

Reaction equation

HRID 860998 reaction equation
[CH3:1][S:2]([C:5]([C:8]1[CH:9]=[C:10]2[C:15](=[C:16]([C:18]3[CH:19]=[C:20]([C:24]4[CH:29]=[CH:28][C:27]([CH:30]=[CH:31][C:32]([OH:34])=[O:33])=[CH:26][CH:25]=4)[CH:21]=[CH:22][CH:23]=3)[CH:17]=1)[N:14]=[CH:13][CH:12]=[CH:11]2)([CH3:7])[CH3:6])(=[O:4])=[O:3].[N+:35]([C:38]1[CH:43]=[CH:42][C:41](O)=[CH:40][CH:39]=1)([O-:37])=[O:36]>CCOCC>[N+:35]([C:38]1[CH:43]=[CH:42][C:41]([O:33][C:32](=[O:34])[CH:31]=[CH:30][C:27]2[CH:26]=[CH:25][C:24]([C:20]3[CH:21]=[CH:22][CH:23]=[C:18]([C:16]4[CH:17]=[C:8]([C:5]([S:2]([CH3:1])(=[O:4])=[O:3])([CH3:7])[CH3:6])[CH:9]=[C:10]5[C:15]=4[N:14]=[CH:13][CH:12]=[CH:11]5)[CH:19]=3)=[CH:29][CH:28]=2)=[CH:40][CH:39]=1)([O-:37])=[O:36]

Participants

4

Reactant 2

HCID 9804-NitrophenolHCID 69374060HCID 69374060, compound

Product 1

HCID 69374630HCID 69374630, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Prepared according to the procedure described in EXAMPLE 11, Step 3 but using 3-(3′-[6-(1-methanesulfonyl-1-methyl-ethyl)-quinolin-8-yl]-biphenyl-4-yl)-acrylic acid and 4-nitro-phenol as starting materials. Stirring in Et2O afforded the title compound after filtration.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-6fb48bda9bac41bba69e0ddc0274dd61
Source dataset
uspto-grants-2006_12
Patent number
US07153968B2

Reaction notes

Loading…