Allyl bromide → N-allyl-N-(2-hydroxyethyl)benzenamine

HRID 861266Notes

Reaction equation

[NH:1]([CH2:8][CH2:9][OH:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:11](Br)[CH:12]=[CH2:13]>>[CH2:13]([N:1]([CH2:8][CH2:9][OH:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[CH:12]=[CH2:11]

Participants

Reactant 2

HCID 7841Allyl bromide

HCID 31235N-(2-Hydroxyethyl)aniline

Product 1

HCID 19702677N-allyl-N-(2-hydroxyethyl)benzenamine

Procedure

2-anilinoethanol (13.7 g, 0.10 mol) is treated with allyl bromide (18.15 g, 0.15 mol), in the manner as set forth in Example 3, to provide N-allyl-N-(2-hydroxyethyl)benzenamine.

Sources & evidence

ORD record: ord-c59f5aed44fb4c66990e59519dcca17b
Source dataset: uspto-grants-1998_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05714304

Reaction notes

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