Ethyl Glycolate → HCID 19702830, compound

Participants

Reaction Conditions

Reaction Steps

A reactor was charged with 10.7 g (0.03 mole) of 15-hydroxy-13,17-diazanonacosan, 50 ml of toluene and 7.1 ml (0.07 mole) of ethyl glycolate, and the contents were heated to 100° C. and continuously stirred for 7.5 hours while purging ethanol formed with a nitrogen stream. After completion of a reaction, the solvent was distilled off under reduced pressure, and the residue was purified by column chromatography (on 200 g of silica gel, developing solvent: chloroform/methanol=100/1), thereby obtaining 13 g (yield: 96%) of the title compound as a viscous liquid.

Provenance & Evidence