HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-cyclohexyl-2,4-dinitroaniline → HCID 5061827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-cyclohexyl-2,4-dinitroaniline | HCID 346027 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 5061827 | HCID 5061827 | 100% |
Reaction Steps
60.0 g (0.23 mol) of N-cyclohexyl-2,4-dinitroaniline were dissolved in 500 ml of tetrahydrofuran and, after addition of 3 g of palladium/carbon (10%), were hydrogenated. The mixture was then filtered and the filtrate was concentrated under reduced pressure to yield 47.2 g (100%) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05714489 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-fdd07337bd114a44ae3e6d89e9886d5b |
| Source note | uspto-grants-1998_02 |