HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 22097137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 22097179 | HCID 22097179 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 22097137 | HCID 22097137 | 98% |
Reaction Steps
24 g (68.6 mmol) of this amide were refluxed in a mixture of 13 ml of concentrated sulfuric acid, 240 ml of water and 250 ml of ethanol for 3 h. The precipitate was then filtered off with suction to yield 16.2 g (98%) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05714489 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-fdade74b5df2442bad1751f04d0fd28e |
| Source note | uspto-grants-1998_02 |