Dimethylformamide → HCID 22097106, compound

Participants

Reaction Steps

8.3 g (35 mmol) of 1-ethyl-6-nitro-2,3(1H,4H)-quinoxalinedione were dissolved in 300 ml of dimethylformamide and, after addition of 2 g of palladium/carbon (10%), were hydrogenated. The mixture was then filtered and the filtrate was concentrated under reduced pressure to yield 5.9 g (81%) of the product.

Provenance & Evidence