Acetyl chloride → HCID 22097143, compound

HRID 861541Notes

Reaction equation

HRID 861541 reaction equation
[CH3:1][O:2][CH:3]1[CH:7]([CH2:8][NH2:9])[CH2:6][CH:5]([O:10][CH3:11])[O:4]1.[C:12](Cl)(=[O:14])[CH3:13]>>[C:12]([NH:9][CH2:8][CH:7]1[CH2:6][CH:5]([O:10][CH3:11])[O:4][CH:3]1[O:2][CH3:1])(=[O:14])[CH3:13]

Participants

3

Reactant 2

HCID 6367Acetyl chlorideHCID 21710167HCID 21710167, compound

Product 1

HCID 22097143HCID 22097143, compound

Procedure

4.0 g of 2,5-dimethoxy-3-aminomethyltetrahydrofuran and 1.75 ml of acetyl chloride were reacted as in Example 89a. 3.7 g of impure product were obtained and were immediately reacted further.

Sources & evidence

ORD record
ord-e946f4be4703485bbf23e2ddafe9c91f
Source dataset
uspto-grants-1998_02
Patent number
US05714489

Reaction notes

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