HCID 19704254, compound → HCID 19704257, compound

HRID 861546Notes

Reaction equation

HRID 861546 reaction equation
[CH2:1]([C:5]1[NH:6][C:7]([C:20](=[O:23])[CH:21]=[CH2:22])=[C:8]([S:10]CC2C=CC(OC)=CC=2)[N:9]=1)[CH2:2][CH2:3][CH3:4]>ClCCl>[CH2:1]([C:5]1[NH:6][C:7]2[C:20](=[O:23])[CH2:21][CH2:22][S:10][C:8]=2[N:9]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 1

HCID 19704254HCID 19704254, compound

Product 1

HCID 19704257HCID 19704257, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

2.1 g of the product of Stage 4 (6.4 mmoles) were dissolved in 65 ml of dichloromethane (10 ml/mmole) and the following were introduced at about 0° C.:

Workup

  1. additionthe following were introduced at about 0° C.

Sources & evidence

ORD record
ord-ab6e20d4e30a4dd4a11cf5ee97cbbcf8
Source dataset
uspto-grants-1998_02
Patent number
US05714508

Reaction notes

Loading…