HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo(d)thiazol-2-amine → N-(benzo[d]thiazol-2-yl)-1H-imidazole-1-carbothioamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo(d)thiazol-2-amine | HCID 8706 | — |
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-(benzo[d]thiazol-2-yl)-1H-imidazole-1-carbothioamide | HCID 19703709 | 44.2% |
Reaction Steps
A solution of 1,1'-thiocarbonyldiimidazole (8.9 g, 50 mmol) and 2-aminobenzothiazole (7.5 g, 50 mmol) in acetonitrile (125 mL) was stirred at room temperature for 20 h. The resulting precipitate was collected by filtration to provide 5.75 g (44%) of the title product:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05714503 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-ebca4691737e49b18fde721bf830f8ef |
| Source note | uspto-grants-1998_02 |