HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyphenethylamine → HCID 19704106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyphenethylamine | HCID 74896 | — |
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19704106 | HCID 19704106 | 53.6% |
Reaction Steps
A solution of 1,1'-thiocarbonyldiimidazole (1.78 g, 10 mmol) and 2-methoxyphenethylamine (1.51 g, 10 mmol) in acetonitrile (25 mL) was stirred at room temperature for 20 h. The resulting precipitate was collected by filtration to provide 1.40 g (53%) of the titled product:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05714503 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-e1b177e5e95c4f159a2e4c0a6feaafef |
| Source note | uspto-grants-1998_02 |