HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzimidazole → N-(1H-benzo[d]imidazol-2-yl)-1H-imidazole-1-carbothioamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzimidazole | HCID 13624 | — |
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-(1H-benzo[d]imidazol-2-yl)-1H-imidazole-1-carbothioamide | HCID 19704123 | 73.3% |
Reaction Steps
A solution of 1,1'-thiocarbonyldiimidazole (8.91 g, 50 mmol) and 2-aminobenzimidazole (6.66 g, 50 mmol) in acetonitrile (50 mL) was stirred at room temperature for 19 hours. The resulting precipitate was collected by filtration to provide 8.92 g (73%) of the titled product:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05714503 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-f77505c6793044cc913761a840942f32 |
| Source note | uspto-grants-1998_02 |