反应详情

Benzyl-3, 6, 9, 12-Tetraoxatridecanoate (5 mmol) is dissolved in methanol (50 ml) and 10% palladium on carbon is added (100 mg catalyst/mmol). The suspension is shaken under 30 psi H2 until the starting material is consumed. The suspension is filtered through a short pad of Celite, washed thoroughly with methanol, and the solvent evaporated. The product is used directly without purification.

1. customis consumed
2. filtrationThe suspension is filtered through a short pad of Celite
3. washwashed thoroughly with methanol
4. customthe solvent evaporated
5. customThe product is used directly without purification