HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridineacetic acid → 3-Piperidineacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridineacetic acid | HCID 108 | — |
| Reactant | 3-Pyridineacetic acid, hydrochloride (1:1) | HCID 2723724 | — |
| Product | 3-Piperidineacetic acid | HCID 283696 | 80.5% |
Reaction Steps
3-Pyridylacetic acid hydrochloride (13 grams) (74.9 mmoles) was hydrogenated as described in Preparative Example 15 to give a mixture of unreacted 3-pyridylacetic acid and the title compound (76:24) (8.63 grams, MH+ 144).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05714609 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-1f1eede3f87642009cca0d54be10fc41 |
| Source note | uspto-grants-1998_02 |