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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 861767Generated: October 30, 2026

Trimethylsilylacetylene → HCID 22619436, compound

https://huagongshe.com/reaction/861767

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrimethylsilylacetyleneHCID 66111—
Reactant6-Bromo-1,1,4,4-tetramethyl-1,2,3,4-tetrahydronaphthaleneHCID 226685—
ProductHCID 22619436HCID 2261943666.1%

Reaction Steps

Following the basic procedure of Example 1(a), by reacting 26.7 g (0.1 mol) of 2-bromo-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene with 20 g (0.204 mol) of trimethylsilylacetylene, 18.8 g (66%) of the expected compound were obtained in the form of a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05716624
Source datasetuspto-grants-1998_02
ORD IDord-ae4d1c1370624aa3a796d8ee1b4ba0c7
Source noteuspto-grants-1998_02