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HRID861801

反应详情

EQUATION

反应方程式

HRID 861801 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1ccc(I)c(C)c1
HCID231757

Methyl 4-Iodo-3-methylbenzoate

C9H9IO2

结构：C#CC(O)c1ccc2c(c1)C(C)(C)CCC2(C)C
HCID11817362

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(C#CC(O)c2ccc3c(c2)C(C)(C)CCC3(C)C)c(C)c1
HCID22619406

未命名化合物

PROCEDURE

实验过程

Following the basic procedure of Example 11(d), by reacting 2.4 g (10 mmol) of α-ethynyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenemethanol with 2.7 g (10 mmol) of methyl 3-methyl-4-iodobenzoate, 3.2 g (83%) of the expected ester, with a melting point of 130°-131° C., were obtained.

WORKUP

后处理

  1. customwith a melting point of 130°-131° C., were obtained