1-Iodohexane → HCID 22619420, compound
Reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([Br:12])[CH:8]=[CH:9][C:10]=1[OH:11])([CH3:4])([CH3:3])[CH3:2].I[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]>>[C:1]([C:5]1[CH:6]=[C:7]([Br:12])[CH:8]=[CH:9][C:10]=1[O:11][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])([CH3:4])([CH3:2])[CH3:3]Participants
3
Procedure
Following the basic procedure of Example 46(a), by reacting 4.58 g (0.02 mol) of 3-tert-butyl-4-hydroxybromobenzene with 3.3 ml (0.022 mol) of 1-iodohexane, 6 g (97%) of 3-tert-butyl-4-hexyloxybromobenzene were obtained in the form of a colorless oil.
Sources & evidence
- ORD record
- ord-03147440a1b34a4b8361dac735eccfa0
- Source dataset
- uspto-grants-1998_02
- Patent number
- US05716624
Reaction notes
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