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HRID861871

反应详情

EQUATION

反应方程式

HRID 861871 的结构方程式

REACTANTS

反应物

2
结构：CC(O)CC(C)O
HCID12262

2,4-Pentanediol

C5H12O2

结构：O=[N+]([O-])c1ccc(CP(=O)(O)O)cc1
HCID5180708

(4-Nitro-benzyl)-phosphonic acid

C7H8NO5P

PRODUCTS

生成物

1
结构：CC1CC(C)OP(=O)(Cc2ccc([N+](=O)[O-])cc2)O1
HCID18928085

未命名化合物

PROCEDURE

实验过程

4-Nitrobenzylphosphonic acid and 2,4-pentanediol were treated in the same manner as in Reference Example 20 to yield 4,6-dimethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide, which was then recrystallized from ethanol-hexane to yield colorless needles having a melting point of 152°-153° C.