HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butyl-2-ethyl-1,3-propanediol → 5-Butyl-5-ethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butyl-2-ethyl-1,3-propanediol | HCID 61038 | — |
| Reactant | (4-Nitro-benzyl)-phosphonic acid | HCID 5180708 | — |
| Product | 5-Butyl-5-ethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide | HCID 18928070 | — |
Reaction Steps
4-Nitrobenzylphosphonic acid and 2-butyl-2-ethyl-1,3-propanediol were treated in the same manner as in Reference Example 20 to yield 5-butyl-5-ethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide, which was then recrystallized from ethanol-hexane to yield colorless prisms having a melting point of 111°-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05716944 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-c4d737db100d4be8abd78afdda316df1 |
| Source note | uspto-grants-1998_02 |